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Catalyst particle shapes and pore structure engineering for hydrodesulfurization and hydrodenitrogenation

《化学科学与工程前沿（英文）》 2022年第16卷第6期页码 897-908 doi: 10.1007/s11705-021-2127-x

摘要： Catalyst particle shapes and pore structure engineering are crucial for alleviating internal diffusion limitations in the hydrodesulfurization (HDS)/hydrodenitrogenation (HDN) of gas oil. The effects of catalyst particle shapes (sphere, cylinder, trilobe, and tetralobe) and pore structures (pore diameter and porosity) on HDS/HDN performance at the particle scale are investigated via mathematical modeling. The relationship between particle shape and effectiveness factor is first established, and the specific surface areas of different catalyst particles show a positive correlation with the average HDS/HDN reaction rates. The catalyst particle shapes primarily alter the average HDS/HDN reaction rate to adjust the HDS/HDN effectiveness factor. An optimal average HDS/HDN reaction rate exists as the catalyst pore diameter and porosity increase, and this optimum value indicates a tradeoff between diffusion and reaction. In contrast to catalyst particle shapes, the catalyst pore diameter and the porosity of catalyst particles primarily alter the surface HDS/HDN reaction rate to adjust the HDS/HDN effectiveness factor. This study provides insights into the engineering of catalyst particle shapes and pore structures for improving HDS/HDN catalyst particle efficiency.

关键词： hydrodesulfurization hydrodenitrogenation particle shape pore structure

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Structural engineering of transition metal-based nanostructured electrocatalysts for efficient water

Yueqing Wang, Jintao Zhang

《化学科学与工程前沿（英文）》 2018年第12卷第4期页码 838-854 doi: 10.1007/s11705-018-1746-3

摘要： Water splitting is a highly promising approach for the generation of sustainable, clean hydrogen energy. Tremendous efforts have been devoted to exploring highly efficient and abundant metal oxide electrocatalysts for oxygen evolution and hydrogen evolution reactions to lower the energy consumption in water splitting. In this review, we summarize the recent advances on the development of metal oxide electrocatalysts with special emphasis on the structural engineering of nanostructures from particle size, composition, crystalline facet, hybrid structure as well as the conductive supports. The special strategies relay on the transformation from the metal organic framework and ion exchange reactions for the preparation of novel metal oxide nanostructures with boosting the catalytic activities are also discussed. The fascinating methods would pave the way for rational design of advanced electrocatalysts for efficient water splitting.

关键词： water splitting structure engineering metal organic framework ion exchange synergistic effect hybrid structure conductive supports

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工程因素对结构振动环境试验响应的影响

陈幼玲,朱学旺,朱长春

《中国工程科学》 2006年第8卷第12期页码 62-65

摘要：

工程因素如试件装配技术状态、试验夹具、控制点位置、载荷控制等对振动试验结构响应的影响一直受到广泛的关注。分析了振动试验中几种主要的工程因素对响应的影响；分析表明，振动试验的识别结果可以预测稳定结构在使用环境下的振动响应。

关键词：复杂结构振动试验结构响应工程因素

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A PDEM-based perspective to engineering reliability: From structures to lifeline networks

Jie LI

《结构与土木工程前沿（英文）》 2020年第14卷第5期页码 1056-1065 doi: 10.1007/s11709-020-0636-1

摘要： Research of reliability of engineering structures has experienced a developing history for more than 90 years. However, the problem of how to resolve the global reliability of structural systems still remains open, especially the problem of the combinatorial explosion and the challenge of correlation between failure modes. Benefiting from the research of probability density evolution theory in recent years, the physics-based system reliability researches open a new way for bypassing this dilemma. The present paper introduces the theoretical foundation of probability density evolution method in view of a broad background, whereby a probability density evolution equation for probability dissipative system is deduced. In conjunction of physical equations and structural failure criteria, a general engineering reliability analysis frame is then presented. For illustrative purposes, several cases are studied which prove the value of the proposed engineering reliability analysis method.

关键词： PDEM reliability structure lifeline networks

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Lightening structure optimization on turbine wheel of vehicular turbocharger

ZHAO Junsheng, MA Chaochen, HU Liaoping

《能源前沿（英文）》 2008年第2卷第4期页码 422-426 doi: 10.1007/s11708-008-0098-y

摘要： Based on basic principle of optimization design, structure optimization of turbine is conducted using optimization module of ANSYS and APDL in order to get the minimum turbine weight. Meanwhile, the original blade profile and flow passage are maintained, and the structural strength of the turbine are guaranteed. Considering assembly technique and cast requirement, the structure of the modified turbine is determined which can save 6.91 percent of the material compared with the original one. The modified turbine not only saved material, but also gained better effect of mass distribution between the turbine and the compressor impeller. The result can provide useful reference to engineering application of turbocharger.

关键词： requirement technique engineering application turbocharger reference

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调整结构　转型发展

杜祥琬

《中国工程科学》 2012年第14卷第3期页码 4-7

摘要：

在经历了30年高速发展之后，我国已进入了一个调整结构、转型发展的关键期。笔者分析了在GDP(gross domestic product)结构、分配结构、产业结构、能源结构等方面存在的问题和结构调整的方向。在此基础上阐述了转变发展方式的内涵和必要性，以及转变发展方式的五个坚持。指出：不良的经济增长会损害未来，战略机遇期首先是转变发展方式的机遇期。转变发展方式必须转变政绩观，改进政绩评价体系。最后，提出了工程领域转型发展的几个方向。

关键词：调整结构转型发展工程领域

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Engineering the electronic and geometric structure of VO/BN@TiO heterostructure for efficient aerobic

《化学科学与工程前沿（英文）》 2023年第17卷第3期页码 276-287 doi: 10.1007/s11705-022-2242-3

摘要： Particle size governs the electronic and geometric structure of metal nanoparticles (NPs), shaping their catalytic performances in heterogeneous catalysis. However, precisely controlling the size of active metal NPs and thereafter their catalytic activities remain an affordable challenge in ultra-deep oxidative desulfurization (ODS) field. Herein, a series of highly-efficient VO_x/boron nitride nanosheets (BNNS)@TiO₂ heterostructures, therein, cetyltrimethylammonium bromide cationic surfactants serving as intercalation agent, BNNS and MXene as precursors, with various VO_x NP sizes were designed and controllably constructed by a facile intercalation confinement strategy. The properties and structures of the prepared catalysts were systematically characterized by different technical methods, and their catalytic activities were investigated for aerobic ODS of dibenzothiophene (DBT). The results show that the size of VO_x NPs and V⁵⁺/V⁴⁺ play decisive roles in the catalytic aerobic ODS of VO_x/BNNS@TiO₂ catalysts and that VO_x/BNNS@TiO₂-2 exhibits the highest ODS activity with 93.7% DBT conversion within 60 min under the reaction temperature of 130 °C and oxygen flow rate of 200 mL·min^–1, which is due to its optimal VO_x dispersion, excellent reducibility and abundant active species. Therefore, the finding here may contribute to the fundamental understanding of structure-activity in ultra-deep ODS and inspire the advancement of highly-efficient catalyst.

关键词： oxidative desulfurization boron nitride vanadium MXene intercalation confinement

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Enhanced photoelectrochemical water splitting with a donor-acceptor polyimide

《能源前沿（英文）》 doi: 10.1007/s11708-023-0910-8

摘要： Polyimide (PI) has emerged as a promising organic photocatalyst owing to its distinct advantages of high visible-light response, facile synthesis, molecularly tunable donor-acceptor structure, and excellent physicochemical stability. However, the synthesis of high-quality PI photoelectrode remains a challenge, and photoelectrochemical (PEC) water splitting for PI has been less studied. Herein, the synthesis of uniform PI photoelectrode films via a simple spin-coating method was reported, and their PEC properties were investigated using melamine as donor and various anhydrides as acceptors. The influence of the conjugate size of aromatic unit (phenyl, biphenyl, naphthalene, perylene) of electron acceptor on PEC performance were studied, where naphthalene-based PI photoelectrode exhibited the highest photocurrent response. This is resulted from the unification of wide-range light absorption, efficient charge separation and transport, and strong photooxidation capacity. This paper expands the material library of polymer films for PEC applications and contributes to the rational design of efficient polymer photoelectrodes.

关键词： polyimide (PI) film photoelectrochemistry band structure engineering aromatic unit

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Consistency Guarantees for Professional Appraisal of Geotechnical Engineering Design under Market Leading

Jian-ye Zheng

《工程管理前沿（英文）》 2015年第2卷第1期页码 82-85 doi: 10.15302/J-FEM-2015012

摘要： Peer review is central to the process of modern engineering. Open peer review gives the impression that decisions are arrived at in a fair and meritocratic manner with an objective, reliable, consistent process. It is responsible for identifying methodological flaws and for improving the quality. Assistance from somebody in the same discipline is valuable. Clients refer to reviewers as referees since they help to determine the fate of a design. The client sets up a hanging committee to carry out open peer review to decide whether a piece of work should be accepted, revised or rejected. Reviewers in similar specialties make up a professional group. In an open peer review refereeing a retaining and protection structure design of building foundation pit excavation, an outside expert as an assessor, might master the art of review to pay attention to guarantee consistency of processes and outcomes.

关键词： peer review foundation pit excavation retaining and protection structure design introduction

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Design of a shaking table test box for a subway station structure in soft soil

YANG Linde, ZHENG Yonglai, ZHANG Dongliang, JI Qianqian, YANG Chao

《结构与土木工程前沿（英文）》 2007年第1卷第2期页码 194-197 doi: 10.1007/s11709-007-0022-2

摘要： A reasonable choice of structure of a model box is significant for a shaking table test to be successful in geotechnical engineering. A model box has been designed for the shaking table test of a subway station structure in the soft soil of Shanghai in the paper. The reasonable geometric similarity scale of the subway station structure has been determined by a 3-D dynamic analysis under the action of lateral equivalent static loading. The shape, size and structure of the model box are chosen by considering all the involved factors comprehensively. The shape of the box is similar to that of a typical station structure, and the ratio between the plane dimension of the model ground and that of the model structure is big enough to reduce the influence of boundary condition effectively. The structure is strong enough to avoid being demolished by shaking during a test. The contact conditions between the model soil and box are clear to help the data gained from the test well fit that from numerical analysis. The total weight of the model soil and box is less than the bearing capacity of the shaking table apparatus and there is no resonance between the model soil and box. The results show that the model box can be used to simulate the dynamic response of a subway station structure very well, so it provides a firm foundation for the success of the shaking table test of a subway station structure.

关键词： geotechnical engineering numerical analysis weight dynamic analysis Shanghai

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Value Engineering/Value Management Model and Application of Aerospace Projects

Wan-hua Qiu,Han-peng Zhang,Ze-Shui Xu,De-Sheng Wu

《工程管理前沿（英文）》 2015年第2卷第4期页码 373-377 doi: 10.15302/J-FEM-2015056

摘要： This paper presents a new space model developed by general value engineering/value management model. The authors take the function analysis, function optimization and function realization of the development object as the basic point, to get the final optimization structure by value evaluation, so as to improve the project quality and reduce the project cost. The final case shows that the application of this model can save about 18% of the time and considerable cost of the usually planned projects under the condition of quality assurance.

关键词： aerospace project value engineering value optimization value stream design structure matrix

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Structure controlling and process scale-up in the fabrication of nanomaterials

Chunzhong LI,

《化学科学与工程前沿（英文）》 2010年第4卷第1期页码 18-25 doi: 10.1007/s11705-009-0305-3

摘要： Nanotechnology is already having a significant commercial impact, and will very certainly have a much greater impact in the future. The research on process engineering and scale-up will be very important for the commercial production and application of nanomaterials, because the properties and structure of nanomaterials are not only determined by the nucleation and growth process, but also strongly affected by the engineering properties, such as the mixing, the heat and mass transfer, and also the distribution of temperature, concentration, etc. This paper will present some research work in our laboratory on the fabrication of nanomaterials. Based on the chemical engineering principle and methods, many kinds of novel nanomaterials can be synthesized and their structure can be easily controlled through adjusting the parameters of the fluid mixing, and the distribution of temperature, residence time and concentration, etc. By using the micro-mixing, heat and mass transfer and reaction control methods, the host-guest nanocomposites have been assembled and assumed as the novel electroanalytical sensing nanobiocomposite materials. Based on the principles of chemical engineering, the manufacturing technologies for magnetic powders, calcium carbonate, and titanium dioxide have been developed for commercial-scale production, and the largest production scale has reached 15 kt/year.

关键词： scale-up significant commercial electroanalytical engineering laboratory

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概念加固思想及工程应用

段敬民,钱永久,张方,曾宪桃

《中国工程科学》 2005年第7卷第8期页码 22-25

摘要：

提出了工程结构加固中新的思路——概念加固。概念加固是运用人的思维和判断，从宏观上决定工程加固中的基本问题、基本概念及基本原则，并阐述了基于“概念加固”思想指导下的整体预应力加固技术，介绍了在工程加固中的应用实例。

关键词：工程结构概念加固整体预应力加固技术

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普光气田钻井井身结构优化设计及管材优选技术

王春江,杨玉坤

《中国工程科学》 2010年第12卷第10期页码 39-43

摘要：

普光气田是我国迄今发现的最大的高酸性整装气田，但由于其地质环境异常复杂，目的层深且存在“斜、塌、喷、漏、硬、毒”等世界级工程技术难题，钻井难度大且风险高。分析了普光气田复杂的地质特点，提出了井身结构优化设计和管材优选思路。根据开发认识的加深及要求论述了4种相应井身结构优化方案，介绍了应用效果并作了相应分析。通过井身结构优化设计实现了用尽可能少的套管程序封隔地层的必封点，提供尽可能大的完井井眼，以保证固井质量和满足高产需求，从而最终实现安全、经济的开发目的。

关键词：普光气田钻井井身结构优化设计管材优选

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老矿区转型发展工程哲学思考

金智新

《中国工程科学》 2014年第16卷第10期页码 64-70

摘要：

老矿区的转型发展是一项复杂的系统工程，必须站在工程哲学的高度总揽全局，遵循工程―自然―科学―技术―产业―经济―社会的协调统一。工程是科技创新的主体，依靠科技进步推动工程创新，工程促进科学、技术、产业、经济、社会的发展。工程要以生态保护为前提，经济促进生态工程建设。稀缺炼焦煤资源的保护与开采是矛盾的对立与统一体，炼焦煤生产企业要兼顾眼前利益与长远利益，特别是老矿区，要解决好资源稀缺性与需求激增性矛盾，实行限量开采，增加资源的回收率，实行以煤为基，资源高效循环利用的大、纵、深产业群建设。现有的安全管控高投入与安全事故频发的矛盾促进了安全理论与技术的发展，安全理论与技术由系统安全到结构安全的转变是事物发展的必然。

关键词：工程哲学不对称开发绿色迁移大纵深产业群保护性开采安全结构理论